Find Pressure Regulator, Tube Fittings, Solenoid Valve on Industry Directory, Reliable Manufacturer/Supplier/Factory from China.

Inquiry Basket (0)
Home > Industry Information > Large laboratory nitrogen generator process and purity requirements

Large laboratory nitrogen generator process and purity requirements

2021-05-02

The large-scale laboratory nitrogen generator uses a low-pressure process to extract pure oxygen and pure nitrogen from the air by deep freezing and rectification, that is, to liquefy the air by the principle of a turboexpander refrigeration cycle, according to liquid oxygen and liquid nitrogen. The boiling point is different, and secondary rectification is carried out in the fractionation column to obtain 99.6% purity oxygen and 99.99% purity nitrogen. Partial liquid oxygen, liquid nitrogen and medical oxygen can also be obtained by changing operations as needed.
Introduction to the process flow of a large laboratory nitrogen generator:
1. Air compressor: The air is compressed by air compressor to 0.5Mpa-0.7Mpa.
2. Pre-cooling: The air is pre-cooled to 5 °C - 10 °C in the pre-cooling unit, and the water is separated.
3. Purification: The air removes residual moisture, carbon dioxide and hydrocarbons from the molecular sieve purification gas.
4. Air expansion: The air expands and cools in the expander to provide the required cooling capacity.
5. Heat exchange: The air is exchanged with the refluxing oxygen, nitrogen, and nitrogen in the main heat exchanger of the fractionation tower, and is reheated to the ambient temperature by the cooled sewage nitrogen.
6. Too cold: The night sky and liquid nitrogen are too cold in the subcooler by nitrogen and nitrogen.
Rectification: The air is rectified and separated in the lower column, and the product nitrogen is obtained at the top of the upper column, which is obtained in the upper column.
Nitrogen gas purity requirements
It can only be filled with nitrogen. At an ambient temperature of 20 °C / 68 °F, the standard pressure of the accumulator in Hebei nitrogen generator is 55kg/cm2/780PSL, and nitrogen should not be overfilled. Precautions for charging the accumulator in the psa nitrogen generator When filling the nitrogen, it is necessary to use a Pressure Gauge, a liquid nitrogen nitrogen generator, and when filling the accumulator with nitrogen, make sure that the accumulator body is intact and that the plug is fully tightened. . Confirm that the switch and relief valve of the pressure gauge are completely closed; after unscrewing the plug on the accumulator, tighten the inflation valve; confirm that the o-ring on the coupling is installed and plug the accumulator After removing it, connect it to the three-way valve and tighten the nut.
The growing demand for carbon molecular sieves will further fuel the industry, and the industry will become well known in an unfamiliar industry in the next few years. Secondly, with the increase of application depth, the requirements for nitrogen production, nitrogen recovery rate, bulk density and compressive strength of carbon molecular sieves are getting higher and higher. Laboratory nitrogen generators will further improve product performance indicators. The general trend of future development of an industry.
Therefore, microelectronic devices, biotechnology products and instruments have strict requirements on the purity of process gases. The requirements for nitrogen production in pharmaceutical production are used for potting of injection. The nitrogen produced by the nitrogen generator does not contain dust and heat. The purity of nitrogen required to produce nitrogen is 99% to 99.99%. Nitrogen is required in the production process. Maintain constant pressure supply to ensure normal operation of production.

Gamma lab nitrogen generator is suitable for lab use, it makes use of pressure swing adsorption technology, separating and collecting nitrogen from air. It is easy to operate, plug and play, one simple push on starting button, nitrogen generator begin to work.

Mini Lab Nitrogen Gas Plant

Laboratory nitrogen generator is one kind of cabinet nitrogen generator.  Its size is within 850 x 920 x 1100 mm, weight within 155 kg. Its details are as below:


2 Detailed technical specification


2.1 Compressed air consumption

The generator consumes a maximum of 115 slpm of compressed air to generate the required N2 flow. Air source is not included in this product.

 

2.2. Air supply pressure

Minimum air supply pressure shall be externally regulated to 600 kPa.  

 

2.3. Air quality

This Generator is provided with one full set of FESTO filters, the air supplied to the Generator still need to be dry and oil-free.

 

2.4. N2 output

2.4.1. Quantity of N2 generate: the generator is capable of deliver 25 slpm nitrogen.

2.4.2. Delivery pressure: the generator delivers N2 at a pressure greater than 450 kPa.  

2.4.3. O2 contamination level: O2 level in the N2 stream is not exceed 0.5%, and does not vary from peak to trough by more than 5% of the absolute concentration.

  

2.5 Dimensions

With package, the Generator size: 850 mm (Length)x 920 mm (width)x 1100 mm(height).  

 

2.6 Weight

With package, the Generator weight is not more than 155 kg.

 

2.7 Wheels

The Generator is fitted with 2 fixed wheels at the rear and 2 swivel wheels with brakes at the front

 

2.8 Connection to power supply

The Generator has a panel mounted connector on the rear panel

• Current capacity at maximum temperature 2.5A<Imax<3.5A ( the power supply is capable of supplying 2.5A nominal)

• Jack plug, 5.5 x 2.5 x 9.5 mm, positive on the centre pin

• Maximum operating voltage at maximum temperature 30VDC.  

• Minimum number of insertions/extractions while maintaining contact resistance specification AND without mechanical failure: > 5000  

• Maximum contact resistance after specified minimum insertions: 30milliohms maximum  

• Insulation resistance: min 100MegaOhms after environmental and durability tests  

• Dielectric withstand Voltage : Min 500V for 60s

• Operating temperature range: -20 deg C to +70 deg C   

 

2.9 Indicator

The Generator has a pushbutton illuminated switch on the front panel

• Button to be flush mounting or recessed into a bezel to avoid damage

• High corrosion resistance, either plastic or stainless steel body  

• No symbol on button

• Size of button and bezel to be ~ 22mm to 30mm

• Mechanical Endurance : > 1000000 activations without mechanical failure

• Electrical Endurance : > 100000 cycles at maximum current and maintaining maximum specified contact resistance• Action mechanism : push on – push off

 

• Current handling capability : 4A DC min break, 4A DC min Make, inductive load (double the maximum expected current demand to give good lifetime)

• Maximum DC Working voltage : at least 40V DC

• Illumination type and color : LED, green

• Illumination Operating voltage: 24VDC

• Operating Temperature Range: -20deg C to +70 degC

• Terminal type : either screw terminal or 6.5mm spade type terminals  

 

2.10. Solenoids

The solenoids on the gas control valves is 24 VDC.

 

2.11. Operation

2.11.1. Operating cycle

A typical operating cycle for the Generator is 1 start per day and then run for 8 hours per day, which is equivalent to 2000 hours of operation per year. Depending upon the particular site, operating time could be anywhere between 0 and 24 hours per day.  

2.11.2. Operation at shutdown

When the power is turned off, the pressure vessels is maintained in the pressurized state by closing the two exhaust valves.  

 

2.12. Start up

2.12.1. Start up time

Start up times means the time from start up to producing qualified nitrogen.

The time to complete start up is less than 15 minutes.  

 

2.13. Gas connections

The two external gas connections on the Generator, Air In and N2 Out, are constructed from brass and are to suit ¼" (6.35 mm) OD tubing. There are labeling in English next to these connections, [Air In" and [N2 Out", as part of the rating label.

 

2.14. Environmental requirements

2.14.1. Operating temperatures

The Generator is normally operated within performance specification over the temperature range:

10ºC - 35ºC from 0 – 3000 m, and 10ºC - 25ºC from 3000 – 4500 m

The Generator can operate safely over the temperature range:

5ºC - 35ºC from 0 – 3000 m, and 5ºC - 25ºC from 3000 – 4500 m

 

2.14.2. Noise level requirements

Noise level from the Generator is less than 72dBa at 1m distance. This is achieved by fitting silencers on the exhaust vents.

 

2.15. Life Requirements

The Generator can operate with a mean time between failure of 5 years minimum.


Lab Use Nitrogen Generator, Laboratory Nitrogen Generator, Laboratory Nitrogen Gas Generator, Laboratory Use High Purity Nitrogen Generator
Wofly Technology Co., Ltd. http://www.gammagases.com